GCMS unknowns analysis results for sample AD27951, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC1901\27951.D Vial: 7 Acq On : 20 Dec 2001 9:37 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.58 1.13 ng/uL 395894 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan e 100 C6H120 000591-78-6 91 2 2-Hexa one 100 C6H120 000591-78-6 91 3 2-He none 100 C6H120 000591-78-6 91 4 2-H< anone 100 C6H120 000591-78-6 91 Abundance Scan 189 (6.575 min): 27951 .D (-) m/ z 43.10 100.00% 43 58 5000 ------------------------- 39 53 | 71 85 100 6.20 6.40 6.60 6.80 7.00 mmmp .. TH mPmTT mmmp m/z 58.10 53.01% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386:2-Hexanone 43

------............ 5000 58 TTT 6.20 6.40 6.60 6.80 7.00 29 m/z S’) .10 17.95% 71 85 190 " r " ■ i' m . ............. I' n m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1553; 2-Hexanone « TTnnnanTmtrtt 6.20 6.40 6.60 6.80 7.00 58 5000 m/z 41.10 16.53%

27 39 ; 71 85 100 "ITUTTguT TITT TTTTT -TTT । HU p m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384: 2-Hexanone 43 6.20 6.40 6.60 6.80 7.00 m/z 100.. 15 8.50% 5000 58 29 39

miz-> .... 4 m 85 mmmm 100 71 ITuTr TT । n 111 TTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ‘ i ■ ■ ■ ■ t 6.20 6.40 \/ ■ ■ । ■ ■ • ■ । ■ ■ ■ ■ ।' 6.60 6.80 7.00

27951.D NP112701.M Fri Dec 21 09:58:31 2001 Page 2

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