GCMS unknowns analysis results for sample AD27951, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27951.D Vial: 7 Acq On : 20 Dec 2001 9:37 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstCoric Area Relative to ISTD R.T.

6.47 0.61 ng/uL 215601 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 .Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H12O 000589-38-8 86 4 3-Hexanone 100 C6H120 000589-38-8 56 Abundance Scan 177 (6.465 min): 27951.D (-) m/z 43.10 100.00% 43 57

A 5000 71

100 39 6.20 ' ) 6.40 6.60 6.80 .......... TT ‘‘"‘ I | ' ■ ' | TT1 I H‘ । ' 0m1 —I 1 , —‘1111TT | _____ ‘‘TTTTTI 4______ §5_____________ ‘TTTTT —mri m/z !57.10 87.76% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #63358: 3-Hexanone 43

5000 57

71

100 -A 4 NAA r । _____ 6.20 J 6.40 6.60 6.80 m/z 71.05 49.55% 85 r • • ’ i1 • • ‘ 11 •" i *'" i r1" i—mm H — 1 "‘‘‘11 TIT m/z->____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357;3-Hexanone 43 — I 57 29 6.20 6.40 6.60 16.80 5000 71 m/z 100.15 27.43% 100

5 ■" i'1 H i " " i" H i" " i"111" " i ■"' 111" r ■ ■ ■ iH HI"1' I" "I1"1111" ||"1 t " 111111 p miz-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #1528: 3-Hexanone \ 4 43 57 ____ 6.20 6.40 6.60 6.80 m/z 41.05 26.64% 29 71 5000 100

. ‘ ... .... 1 .... TOIVU1011010TEIOVTCOU00E . —‘0UOV0Iu0VuII .... —OOIOTOOII 85_____ .____ —w0W]VCOOVCPTVOCTTT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27951.D NP112701.M Fri Dec 21 09:58:29 2001 Page 1

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