GCMS analysis report, Jan 2002

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Data File : C:\HPCHEM\l\DATA\DEC2101\28172.D Vial: 38 Acq On : 22 Dec 2001 2:53 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

6.40 0.45 ng/uL 108798 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 91 4 3-Hexanone 100 C6H120 000589-38-8 53 Abundance Scan 170 (6.399 min): 28172.D (-) m/ Z 43.10 100.00% i 43 57 l

71 5000 100 A AAA • I1 6.00 • l r' ■ f I1 111 1 1I 6.20 6.40 6.60 6.80 — +.—85. — + i""r"'i • ■ I ■ ■" i m/z 57.10 93.25% miz-?20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone A 43

5000 57

71

100 —Ar 6.00 _ A_ 6.20 6.40 6.60 6.80

rrrrprrrrp- I" " P 1 I 85 'I1......... 'I H.. p "' I prr m/z 71.05 56.52%

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57 ■ I —4 6.00 6.20 6.40 6.60 6.80 29 71 5000 m/z 100.15 28.70% 100 I . 85 p 1111 I'" ’I ‘" I ।■•■•। ।• IOT— ■ ■i " i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 1........ \ \...... 43 6.00 6.20 6.40 6.60 6.80 57 29 m/z 41.10 25.42% 5000 71

m/z-> _ ......... ................ ....... 85........ ' ' " r ’ I'!' i - ■ i •' 11" " i "1' r C‘T‘TTTT‘1111“TVIWIITIOTTTpr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 AMA 6.00 6.20 6.40 6.60 Ar 6.80

28172.D NP112701.M Fri Dec 28 09:08:13 2001 Page 1

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