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GCMS analysis report, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS results for sample AD28171 analyzed on January 2, 2002.

NYC-WTC_000035365–000035380

Folder label: “GCMS X 11/26/01 A 12/22/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28172.D Vial: 38 Acq On : 22 Dec 2001 2:53 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.50 0.85 ng/uL 207796 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 000591-78-6 91 Abundance / Scan 181 (6.500 min): 28172.D (-) m/z 43.10 100.00% । i i 43 i 58 5000-

100 PrrTTr 6.20 AXA_ 6.40 6.60 6.80 1 T’TTTTTTTTT ■' i + ITTmtr t । ■ ■38 TTTTTTTTTTT 85 71 — i ‘ •1' i — r " • i m/z 58.10 55.80% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385: 2-Hexanone 43

5000 58 — ------1 — 620 6.40 6.60 6.80 29 m/z 57.10 18.89% 39 71 85 100 I m/z--> i i ■1 ■1111 TTTPTTT mm +TTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 l •" ' I F I'1 ’ ’ i

Abundance #1556: 2-Hexanone i 43 A- -4 ' ' I ' ' ' ' I 6.20 6.40 6.60 6.80 58 5000 m/z 41.10 18.37%

27 39 71 85 100 r"•i i 11. l T’T r " • i IT T‘ECTTU1"TT"TTT‘TTTT TTTN

A " I *'1 I" " I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance I #63384: 2-Hexanone A-PI 43 6.20 6.4C 6.60 6.80 m/z 100.15 9.82% 5000 58 . 29

m/z-> -H - -7l 39 11........... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 85 100 TCTTTu ----- 6.20 6.40 6.60 6.80

28172.D NP112701.M Fri Dec 28 09:08:15 2001 Page 2

NYC-WTC_000035374

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NYC-WTC_000035374Source: NYC Law Department, mirrored locally

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