GCMS analysis report, Jan 2002

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Data File : C:\HPCHEM\l\DATA\DEC2101\28172.D Vial: 38 Acq On : 22 Dec 2001 2:53 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol, (R)- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.75 0.57 ng/uL 138623 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol, (R) - 102 C6H140 026549-24-6 83 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 83 3 2-Hexanol 102 C6H140 000626-93-7 83 4 2 -Hexanol 102 C6H140 000626-93-7 78 Abundance Scan 208 (6.747 min): 28172.D (-) m/z 45.10 100.00% / 45

5000 ------------- ■ • i ■ • ■ ■ । ■ . 69| 6.40 6.60 6.80 7.00

m/; TTTTTT mm 56 87 T*—u"gn 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 207 TTTTTT m/z 41.10 16.35% Abundance #1794: 2-Hexanoi, (Rj- I

5000 45

69 AA 6.40 m/ z 6.60 43.10 6.80 ' ' I ' ' ' ' I ' 7.00 13.75% 29 1 ।। 19 ।। "ITT 11111» 55 i"" i 1 i"87 "i ।. > > 11 rn 11.»।. 11.. 111 ■ 11111 TTT’T 11111 ■ 11111111111111«11

m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 'Abundance #63545: 2-Pentanol. 4-methyl- 45 A6.40 TT11n 6.60 6.80 7.00 IT

5000 - m/z 69.10 13.48% 69 27 57 87 I'"' I i1i i ■ ■" । TTTTTJTTT‘l—EE10—E011"T7I0"T271"I1"1"‘‘‘IE—‘-1-0T0"TTII"TT m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #63583: 2-Hexanol IT 45 6.40 6.60 6.80 7.00 m/ z 44.10 9.84% 5000-

AA 4 I 27 — 69 m 55 1 TTTTTTTTTT 87 A TT m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 6.40 6.60 6.80 7.00

28172.D NP112701.M Fri Dec 28 09:08:17 2001 Page 3

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