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GCMS analysis report, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS results for sample AD28171 analyzed on January 2, 2002.

NYC-WTC_000035365–000035380

Folder label: “GCMS X 11/26/01 A 12/22/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC21O1\28172.D Vial: 38 Acq On : 22 Dec 2001 2:53 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.77 3.80 ng/uL 923792 1,4-Dichlorobenzene-d4 11.79

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

4 -hydroxy-4 -me thyl- 1 2 - Pentanone , 116 C6H1202 000123-42-2 59 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 53 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 43 4 Acetic, acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 28 Abundance Scan 319 (7.765 min): 28172.D (-) 43 m/ z 4 3.10 100.00%

59 5000

101 53., | — 7.40 7.60 7.80 8.00 8.20 ____ ____ I ‘ ■ 1 1 i ■ ■ • ■ i ■ ' ■ 1 I' III+ 3&469 83 TIT ' 1 i ''' 1 ’ i m/ z 59.10 49.54% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00___ 8.20 m/z 101.05 17.71% 15 31 101 | I I 83 I I ' • • ' I ' ‘ ‘ ' I ' ""d I ' ' ' • l • • - 'I T’T miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

7.40 7.60 7.80 8.00 8.20 5000 m/z 58.10 16.34% 59 i ■

101 i ‘ ‘ ' i 1 271 ■ ' ■ i ' ' ■ ■ i ' ■ 49 ' ' i ' ' ' I 1 i ' ■ ■ ' i 83 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- I 43 7.40 7.60 7.80 8.00 8.20 m/ Z 41.10 7.03% 5000 59

31 —...................... ....................................... I I । I Il|............... 73 , ............... ; 101 893 | i ' ' ■ ■ i ' ■ ' ' i ' —I+ — m/z-> 10 20 30 40 50 ।60 70 80 90 100 110 7.40 7.60 7.80 8.00 8.20

28172.D NP112701.M Fri Dec 28 09:08:19 2001 Page 4

NYC-WTC_000035376

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NYC-WTC_000035376Source: NYC Law Department, mirrored locally

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