GCMS analysis report, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2101\28309.D Vial: 41 Acq On : 22 Dec 2001 5:37 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.51 0.78 ng/uL 203348 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2 - Hexanone 100 C6H120 000591-78-6 91 3 2-He none 100 C6H120 000591-78-6 90 4 2-Hexanone 100 C6H120 000591-78-6 86 Abundance Scan 182 (6.507 min): 28309.D (-) m/ z 43.1,0 100.00% 43 58 5000

TT 100 6.20 6.40 6.60 6.80

m/z-> yn rq n r. । rr.. V 1WWMTTTTT4 71 85 53 | TTITTPPPPWPIWPTTRTT — I' ' " I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/ Z 58.10 53.73% Abundance #63385: 2-Hexanone 43

5000- 58 -n-f-T-r-. TTTT TIIT j 6.20 6.40 6.60 6.80 29 m/z 57.10 17.37% m+ TT H ।।. TTTTTFT ri 11 ii 111111 fror । TT 39 71 85 100 ' ■ i " ■' r ' I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

5000 43 #63384: 2-Hexanone

58 -P-r 6.20 m/ z J 6.40 41.1.0 6.60 ‘rt18—T 6.80 16.92% 29 i 39 85 100 71 TVTTTIWUTTT ' I " ' ' I‘‘11 fTT‘T"‘‘‘1‘‘711 rm-f I ’ • I' 11 •” I i" " i" r' " I " m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386:2-Hexanone \ — 1 . fill)

43 6.20 6.40 6.60 6.80 m/z 39.10 8.35% 5000- 58 29 - 71 85 100 i TTPTT -TTr-p-rrrpr I — ...... I i1'1 ■ । n-p-r i ■1111 1 r ■ ■1 ■ । ■ •1 1 i m/z- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

28309.D NP112701.M Fri Dec 28 09:10:08 2001 Page 1

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