GCMS analysis report, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2101\28309.D Vial: 41 Acq On : 22 Dec 2001 5:37 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.75 0.45 ng/uL 117217 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Pentanol, 4-methyl- 102 C6H140 ______ 000108-11-2 74 Abundance Scan 208 (6.746 min): 28309.D (-) m/z 45.10 100.00% 45

5000

IT 56 69 87 6.40 6.60 6.80 7.00 1 m/z- T’TTTT ll .—— p i ri p i 1111 < 11 {11 » I I

10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190200210 T’TTTT । < I ! p .. I | I .. I | I I I . | i'"1 r 207 t111111 m/ z ■ , 43.10 14.12% Abundance #63584: 2-Hexanol 45

5000- TTTTIGun—reusnuTT 6.40 6.60 6.80 7.00______ 69 m/z 69.10 12.63% 27 h 56 | 87 I'1111 ri r " ■ i ■ P''' I"111''" I'111 p111 p ''' p " ‘ I'' ‘' p' " P ‘" P11 • I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200210 Abundance #63546:2-Pentanol. 4-methyl- 45 AL....... — 6.40 6.60 6.80 7.00 5000 m/z .41.05 11.64% 27 69 57 87 F' ‘ 'T TOTI I" " I TTTTTyTrrrpXTTpTTnYrTTrp-TTTpnnTyrTT^^ m/z--> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #63547: 2-Pentanol, 4-methyl- A— ... i 45 6.40 6.60 6.80 7.00 m/z 44.10 10.16% 5000

27 57 68 87 ..... A I" 111 T TT Th 1*. TT ....P.1.1111111111111111 T’EEIIEETIITTETTE’ITTTTETI’TT ■ ' i ' ■ ■ ' i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110120130140 150160170180190 200 210 7.00

28309.D NP112701.M Fri Dec 28 09:10:10 2001 Page 2

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