GCMS analysis results for sample AD28104, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\DEC2101\28167.D Vial: 17 Acq On : 22 Dec 2001 9:25 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator). Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

6.38 0.52 ng/uL 113280 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 90 3 3-Hexanone 100 C6H120 000589-38-8 90 4 3-Hexanone 100 C6H120 000589-38-8 64 Abundance Scan 168 (6,383 min): 28167.D (-) m/z 43.10 100.00% 43 57

71 5000

w TU—T ।_1_____ 85. ______ 100 6.00 —M 6.20 6.40 6.60 6.80 TTUIDTge +TTTTTTTTTTTt j‘ P1 IM | i. i ij i< “ 'ItIH | m/z 57.10 95.91% miz-? 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358: 3-Hexanone 43 57

5000 71 1154 MV.A 6.00 6.20 6.40 6.60 6.80 100 m/z 71.05 53.20% mmmmmm , 85 HTTT Tpmu—Tguur " r "' i miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance i

29 43 #60357: 3-Hexanone 57 6.00 ’ । 6.20 ■ A 6.40 6.60 6.80 5000 71 m/ z 41.10 27.88% 100

miz-2 Abundance ______________ _______ r । .-m I00I1—m0—; u—' ——i,______ pgT 85_______ _____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 43 #1528: 3-Hexanone 57 A MMJ 6.00 6.20 m/z 100.15 6.40 6.60 27.47% 6.80

29 71 5000 100

miz—> T TTTTTTTHT TTTTTTT 'I........... I' ................ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 tmm i'." i T-p-r-r-T-j-i-r 600 6.20 । ■ ■ ■11 ■ ■1 ■ । 6.40 6.60 6.80 ■

28167.D NP112701.M Fri Dec 28 09:58:03 2001 Page 1

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