GCMS unknowns analysis results for sample AD27952, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27952.D Vial: 8 Acq On : 20 Dec 2001 10:32 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.68 ng/uL 276109 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 87 2 3-Hexanone 100 C6H120 000589-38-8 87 3 3-Hexanone 100 C6H120 000589-38-8 72 4 3-Hexanone 100 C6H120 ____ 000589-38-8 53 Abundance i Scan 178 (6.476 min): 27952.D (-) m/z 43.10 100.00% 43 57 ■

71 5000 100 TTfm 39 ml +3+ *p""i +..........Pm 85 6.20 6.40 6.60 6.80 1 r"'t " ।" i ■ m/ z 57.10 98.80% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43

I 57

5000 29 71 TTTTImt 6.20 6.40 6.60 6.80 100 m/z 71.05 57.09%

m/z-> ... . ........... . " I''' ■ I'' ” I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 tmm Tpp

Abundance #63358:3-Hexanone 43 57 J... AA... 6.20 6.40 6.60 6.80 5000 71 m/z 100.15 30.78% 100

m/z-> "' • I" " I' ■" 11 ■ ■ ■ I • mmmm I I >.. ।........... . . > | > < . | H . > । . . । . H...... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 । > > > (i > H । < TTP..... .

Abundance #63356: 3-Hexanone ■ ' i ■ ' ' • i ' ■ ' ■ i ' ■ 29 43 57 6.20 6.40 6.60 6.80 m/z 41.10 27.81%

. NA 5000 71

100 ..... — .... 38 , ..... ......... . ..... 85....... ..... 1" 111" i1 ' i' " ' i"1' 1 1 111'" i1 “' I' 111" " i" " i 1'11" " i" " i " ■111" ■ 111" 1'" I" " |1 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27952.D NP112701.M Fri Dec 21 10:05:42 2001 Page 1

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