GCMS analysis results for sample AD28104, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28167.D Vial: 17 Acq On : 22 Dec 2001 9:25 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.91 ng/uL 200435 1,4-Dichlorobenzene-d4 11.78

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 90 4 2-Hexanone 100 C6H120 000591-78-6 86 Abundance Scan 179 (6.483 min): 28167.D (-) m/z 43.10. 100.00% 43 58 5000 r '' .. .............. T PrTr 71 85 100 6.20 6.40 6.60 6.80 miz-> mmmm 1—— TTTTT — T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m T m/z 58.10 52.77% Abundance #63385: 2-Hexanone 43

5000 58 ".I III —A 6.20 6.40 6.60 6.80 29 m/ z 41.10 18.36% 39 71 85 100 mm +— +TTTITTTTTHTTTTTTTTWTTTTTTTTTTTTTTTTTTTTTTTTT

M MW 1111' 1"1 miz->__ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 763384 2Hexanone 43

___ 6.20 6.40 6.60 6.80 5000 58 — m/z 57.05 15.23% 29 39 71 85 100 '■ i""r ■"i■ ■ ■ ■ r' "I " " I" ■'r■■ ■ i " ■11■ ■ ■ ■ i■11111"'r '"r TITTTTTTTTTTTTTTTTTTTT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556: 2-Hexanone 43 6.80 m/z 39.1) 8.41% 58 5000

27 39 71 85 100 A.. ...... mpp TTTpuT tmmTT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

28167.D NP112701.M Fri Dec 28 09:58:06 2001 Page 2

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