GCMS analysis results for sample AD28104, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report t Data File : C:\HPCHEM\l\DATA\DEC2101\28167.D Vial: 17 Acq On : 22 Dec 2001 9:25 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.73 0.64 ng/uL 140276 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Rexanol 102 C6H140 000626-93-7 74 4 2 -Hexanol 102 C6H140 _000626-93-7 74 Abundance Scan 206 (6.731 min): 28167.D (-) m/z 45.10 100.00% I 45

5000

41 69 6.40 6.60 6.80 7.00 84 87 - ............... 1..... m/z->__ ;10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 TTTTTT m/z 69.10 15.35% Abundances #1792: 2-Hexanol 45

5000 • ‘ I ‘ ‘ ' I ' 1 ’ p ‘ ’ I ' ' • ' I 6.40 6.60 6.80 7.00

miz->

5000 . 1.. 2731. 3942 “ #63584: 2-Hexanol 45 55 58 69

69 84 87 TTPTTTTTT TWWWIIWTTTITTTTTTTTTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance5... T

84 87 .M m/z ____

’ ’ M r' ' ' I ' ' * ' I

m/z 6.40 41.10

6.60 43.10 6.80 14.23%

........ 14 7.00 13.11%

19 42 J 27,31 56 TTT + m/z-> Abundance 1 11'' ’' 11 1" 111111" " I'' 15 20 25 30 35 40' 45 50 55 60 65 70 75 80 85 90 #63583: 2-Hexanol 45 11 ■' 95 JU6.40 6.60 TTTTTTTm 6.80 7.00 m/ z 44.1,0 10.86% 5000

miz-> PutTTTTTTTTT 27 31 10 15 20 25 30 35 40 45 39 42, 55 58 69 J_________ 84 87 ।1111. ।।. T10unntmu—uu—u—"T‘u‘ 50 55 60 65 70 75 80 85 90 95 AAAL , A l A A 6.40 6.60 6.80 7.00

28167.D NP112701.M Fri Dec 28 09:58:07 2001 Page 3

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