GCMS analysis results for sample AD28168, Jan 2002

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Data File : C: \HPCHEM\ 1 \DATA\DEC2 10128164.D Vial: 14 Acq On : 22 Dec 2001 5:46 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.50 1.16 ng/uL 339078 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2 -Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 000591-78-6 91 Abundance Scan 181 (6.505 min): 28164.D (-) m/z 43.10 100.00% 48

5000

.... 34 1 .......,,53 II hl 58

7111.. ■ ।।85|। 100 6.20 6.40 6.60 m/z 58.1.0 A„ 6.80 52.06% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance ... “ “ .... T #1556: 2-Hexanone 43

58 5000 " I ■ ' "T■ 11............ 6.20 6.40 6.60 6.80 m/ z 57 . it) 17.87% 27 39 71 85 100

miz-> m mm+ ————— 11 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386: 2-Hexanone 43 11 1 I T 6.20 6.40 6.60 6.80 5000 58 m/ z 29 :: 1: 71 85 100 TWIPPTTTTTTTTTT TTgmm । j | [TT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Loo w Abundance #63385: 2-Hexanone 43 6.20 6.40 6.60 6.80 m/z 100.. 15 8.76% 5000 58

29

miz—> m 39 71 85 100 m — +TTTTTTTTTTTT tpTT TITTTTIWTTWWTTWTIWTTTNTOTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ■ ■

6.20 l ■ ■ ■ ■

6.40 l 1 1 ' ■

6.60 I ' ■ ■ ■

6.80 l ■ ■ ■ ■ I

28164.D NP112701.M Fri Dec 28 09:56:21 2001 Page 2

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