GCMS analysis results for sample AD27765, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27765.D Vial: 8 .Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanone Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.45 2.67 ng/uL' 599309 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone/ 100 C6H120 000589-38-8 91 2 3 -Hexanone 100 C6H120 000589-38-8 90 3 3-Hexanone 100 C6H120 000589-38-8 90 4 3-Hexanone 100 C6H120 000589-38-8 64 Abundance Scan 175 (6.446 min): 27765.D (-) m/ z 57.10 100.00% 43 57

71 5000 100 39 6.00 6.20 6.40 6.60 6.80

miz-> r •'11 4 4 Hpp 4PHp 53, 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 84 +T7TTrrTTP m/z 43.10 99.89% Abundance #1528: 3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 6.80 100 m/2 71.0 5 52.59%) 85 " i" ■ ■ i TTTTITTT ..... . *, —pr TOWIR, T1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 43 57 1mmm 29 6.00 6.20 6.40 6.60 6.80 5000 - 71 m/z 41.10 29.80% 100 85 | I"'‘I"1'I""I" "!" ‘T T’’’’T‘ ‘‘ITTTTTT1’0117—q—r,TTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358: 3-Hexanone 43 6.00 6.20 6.40 6.60 6.80 57 m/z 100.15 28.41% 71 5000 -

m/z-> mmmmmmmm 1 — 1' 11"111"11 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 85 TIBpnnir T—Puungur 100

" i1' " i' MA 6.00 6.20 M 6.40 6.60 6.80

27765.D NP112701.M Thu Dec 20 11:23:36 2001 Page 5

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