GCMS analysis results for sample AD27765, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27765.D Vial : 8 Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Furan, tetrahydro-2-(methoxyme Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.10 1.54 ng/uL 345083 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, tetrahydro-2 -methoxymethyl) 116 C6H1202 019354-27-9 59 2 Furan, tetrahydro-2- (methoxymethyl) 116 C6H1202 019354-27-9 45 3 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 42 4 Cyclopentanol, 1-methyl- 100 C6H120 001462-03-9 9 Abundance / Scan 137 (6.097 min): 27765.D (-) m/ z 71.05 100.00% 71

5000 43

1 . , । ri TTIyr । । TTT f1 । 1 ' i 51 57 i 5.80 6.00 6.20 6.40

miz-> 20 i-1-1-1-1-1-1-I । । 1 30 38 40 ' —5051460 —70 81 80 90 100 100 110 120 m/z 43.10 44.48% Abundance #3276: Furan, tetrahydro-2-(methoxymethyl)- 7h 43 s 5000 5.80 6.00 6.20 6.40 m/z 41.10 25. 28% 27 ■ i ■ ■ I | I ■ • i • ■ ■ 'i' 53 58 ■ ' I ■ ' ' ! I ' ' ,........ 116 m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64310: Furan. tetrahydro-2-(methoxymethyl)- 71 — L 43 5.80 6.00 6.20 6.40 5000 m/ z 42.10 19.68%

m/z-> Abundance 20 ; i ■ i > ■ • ■ l • ■ ■ ■ I 1 > 1 1 1 1 ■ ' 1 I 30 40 50 53 58 60 ll i ' ' ' ' i ' 1 1 1 1 1 1 70 #11901: Propanoic acid, 2-methyl-, anhydride 71 80 85 90 100 110 116 120

m/ Z 5.80 JU 1 | 6.00 39.10 ■ I • • r . । . . . . । 6.20 6.40 11, 51% 43 5000

27 U m/z-> • i ■ ■ • • i • I +384 55 tr ‘ i ' ' ' ' i ' ' ————— 20 30 40 50 60 70 80 90 100 110 120 5.80 6.00 6.20 6.40

27765.D NP112701.M Thu Dec 20 11:23:34 2001 Page 4

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