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GCMS analysis results for sample AD26625, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26625 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031920–000031939

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26625.D . Vial: 8 Acq On 6 Dec 2001 4:34 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 2-Furanol, tetrahydro-2-methyl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.12 1.65 ng/uL 534735 1,4-Dichlorobenzene-d4 11.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Furanol, tetr. ydro-2-methyl- 102 C5H10O2 007326-46-7 43 2 Propanoic acid/ 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 40 3 Furan, tetrahydro-2 - (methoxymethyl) 116 C6H1202 019354-27-9 23 4 Cyclopentanol, 1-methyl- 100 C6H120 ________001462-03-9 9 Abundance “ Scan 140 (6.123 min): 26625.D (-) m/z 71.05 "" 100.00% 71

5000- 43

' ' ' । ■ 1 1 1 i ' 1 1 1 n ■n . ।

' m/z->_____ 20 ..................... ■ i ■ ■ ■ ' i ' r ' ' I ' 1 30 40 51 57 I ' 1 1 1 1 1 50 60 d, - ---..,,,,, - 70 80 90 100 110 120 m/z 5.80 6.00 43.10 6.20 6.40

Abundance #63475: 2-Furanol, tetrahydro-2-methyl- 71

5000 43 5.80 6.00 6.20 6.40 m/z 41. 0 24.73% - 49 . 55 61 i . • • • i • . . ......... 84,, miz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance

5000- 43 #11901; Propanoic acid, 2-methyl-, anhydride 71 Am/z 5.80 6.00 42. 1 i 1 ■ 1 ' i 6.40 19.48%

27 I 38 55 ' l ' ' ' ' i ' l ' ' ' ' I ' 1 ' ' i ' ■ ' ' I ' ' ' ■ i 1 ' ' ’ i ' ' ' ■ i ' ' ' ' l ' ' ' ' 1 1 ’ m/z-> 20 30 40____ 50 60 70 80 ____90 100___ 110 120 Abundance #3276: Furan, tetrahydro-2-(methoxymethyl)- — Pr "YMT i 71 5.80 6.00 6.20 6.40 43 m/ z 3 9.00 10.92% 5000

m/z-> 27 1 • i ■ ■ ■ ■ i 20 30 > > _ L 11 1 40 53 58 ’ • i TPT 1 i ■ ■ 50 60 L................ ,116 70 80 90 100 110 120 4. 4 4,44 5.80 6.00 6.20 6.40

26625.D NP112701.M Fri Dec 07 14:48:37 2001 Page 4

NYC-WTC_000031930

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NYC-WTC_000031930Source: NYC Law Department, mirrored locally

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