GCMS results log, sample AD26982, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26982.D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************** * Peak Number 4 Furan, tetrahydro-2-(methoxyme Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.14 0.89 ng/uL 368145 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, tetrahydro-2 -(methoxymethyl) 116 C6H12O2 019354-27-9 59 2 Furan, tetrahydro-2 - (methoxymethyl) 116 C6H1202 019354-27-9 45 3 2-Hepten-3-ol/ 4,5-dimethyl- 142 C9H180 055956-37-1 38 4 Propanoic acid. 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 36 Abundance J Scan 141 (6.137 min): 26982.D (-) m/ z 71.05 100.00% 71

5000 43

miz-> 10 20 30 X -l 40 50 57

60 70 80 #3276: Furan, tetrahydro-2-(methoxymethyl)- 90 100 100 110 120 130 5.80 m/z 6.00 6.20 43 05 6.40 47.03%

Abundance I 71 43 V 5000 Til 5.80 6.00 6.20 6.40 m/z 41.05 25.08% 27 58 i i I!................. 116...... 'i 1'''i ' ■ ■ ■ i ■ ■ ■ ■i' ‘ i ■ ■ ■ ' i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130

W AW Abundance #64310: Furan. tetrahydro-2-(methoxymethyl)- 71 PF 43 5.80 6.00 6.20 6.40 5000- m/ z 42.10 21.81%

f — 1 , 58 85 116 ■ i ■ ■ ■ ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8051: 2-Hepten-3-ol, 4,5-dimethyl- 14 r Tr i PTTYTTT 71 5.80 6.00 6.20 6.40 m/ z 39.10 11.78% 5000 - 43

m/z-> ■

10 15 ' i ' ' ' ■ i

20 27

' ■ ' ■ i ■ ' ■

30 ■ i ' ■ ■ ■

40 i • •

50 55 , । I ! ।— 60 81 100 109 70 80 124 90 100 110 120 130 M 5.80 6.00 \ 6.20 A 6.40 j

26982.D NP112701.M Tue Dec 11 14:48:49 2001 Page 4

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