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GCMS analysis results for sample AD26677, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26677 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031989–000032006

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032000
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\26677.D Vial: 11 Acq On 6 Dec 2001 7:17 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Furan, tetrahydro-2 -(methoxyme Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.12 1.19 ng/uL 334923 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1Furan, tetrahydro-2 - (methoxymethyl) 116 C6H1202 019354-27-9 38 2Furan, tetrahydro-2- (methoxymethyl) 116 C6H1202 019354-27-9 38 32-Hepten-3 -ol, 4,5-dimethyl- 142 C9H180 055956-37-1 38 4Cyclopentanol, 1-methyl-____________ 10 0 C6H12 0 ____ 001462-03-9 38 Abundance ’ Scan 139 (6.119 min): 26677.D (-) i m/z 71.05 100.00% ! 71

5000 43

57 -..— -A 5.80 6.00 6.20 6.40

m/z-> ----- 10 20 30 40 50 60 —511... 1 . 70) TT • 1 ■ 1 । 80 90 । 1 T । ■ iii । । । । r । । 100 110 120 130 100 m/z 43.05 4 4.48% Abundance #3276: Furan, tetrahydro-2-(methoxymethyl)- 7|1

43 5000- 5.80 6.00 6.20 6.40 m/z 41.10 27.41% 27 58 - 4................. ■ ......................... 116 _ • ' I TT • I • ' 70 80 90 100 110 120 130 m/z-> 10 20 30 40 50 60 Abundance #64310: Furan. tetrahydro-2-(methoxymethyl)- 71

43 5.80 6.00 6.20 6.40 5000 m/ z 42.10 21.35%

■ i 1. ■ ■ ■ • i ■ 58 1 ' i ' ' ' ■ i ■ 85 116 m/z-> 10__ 20 30 Abundance 40 50 60 70 80 90 #8051: 2-Hepten-3-ol, 4,5-dimethyl- 71 100 110 120 130

5.80 AAA AAAMAA 6.00 6.20 6.40 m/z 39.00 12.10% 5000 43

27

m/z-> 10 15 . I | . . I l f l <

20 1 30 |

40 , I | ,

50 55

70 ,, । I | , I | | | TEET0 60 81 —0/0/r 1‘1—trE—m—nttir 80 100 109 90 124 100 110 120 130 AA TT r-j-T, . . Tdnnnd.T ) i । ! i i Tf 5.80 6.00 6.20 6.40

26677.D NP112701.M Fri Dec 07 14:52:27 2001 Page 5

NYC-WTC_000032000

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NYC-WTC_000032000Source: NYC Law Department, mirrored locally

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