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GCMS analysis results for sample AD27679, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27679 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033263–000033284

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033274
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27679.D Vial: 6 Acq On : 19 Dec 2001 11:43 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Furan, tetrahydro-2-(methoxyme Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.11 2.51 ng/uL 557273 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, tetrahydro-2-(methoxymethyl) 116 C6H1202 019354-27-9 45 2 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 40 3 2-Hepten-3-pi, 4,5-dimethyl- 142 C9H180 055956-37-1 38 4 Cyclopentanol, 1-methyl-_______ 100 C6H120 001462-03-9 36 Abundance Scan 139 (6.114 min): 27679.D (-) m/z 71.05 100.00% 7|1

5000 43 4 — — ----- A — miz-> ................................. — 10 20 30 40 +L 50 60 701 1................... 100.......................... 80 90 100 110 120 130 m/z 5.80 6.00 43.10 6.20 6.40 45.10% Abundance #64310: Furan, tetrahydro-2-(methoxymethyl}- 71

43 5000 5.80 6.00 6.20 6.40 m/z 41.10 25.96% — TBi 58 ,4....... 85..................... 116....... — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130

W.. 4 - AA Abundance #11901: Propanoic acid. 2-methyl-, anhydride 71 i 5.80 6.00 6.20 6.40 43 5000 m/z 42.10 20.04%

27 37.!, ‘ FTCTr0TFT-IBBS/STIO/O/I/T 55 > । rj ' M . । i ( । i । । । j । . m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8051: 2-Hepten-3-ol, 4,5-dimethyl- 49 71 5.80 6.00 6.20 6.40 m/ z 39.10 11.32%

5000 43

27

miz-> 15 30 55 I I i■ i ■ — ' 1 1 ' 1 ■ < । 1 1 • 1 I ' 1 1 1 i 1 ■ ■ ■ i ■ ‘ 10 20 40 50 60 . . 70 81 80 100 109 —ITT T T 90 100 110 120 124 130 W 4 AAA 5.80 6.00 6.20 6.40

27679.D NP112701.M Thu Dec 20 11:42:08 2001 Page 4

NYC-WTC_000033274

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NYC-WTC_000033274Source: NYC Law Department, mirrored locally

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