GCMS analysis results for sample AD27679, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27679 .D Vial: 6 Acq On : 19 Dec 2001 11:43 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanone Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.45 0.80 ng/uL 178256 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 91 4 3-Hexanone 100 C6H120 000589-38-8 72 Abundance > Scan 176 (6.453 min): 27679.D (-) m/z 43.10 100.00% 43 57

71 5000- 100 6.20 6.40 I6.60 6.80 , 53. 85 i' •" r • • • i TTWII + TIT 111111 11" ‘ I m/z 57.10 94.32% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57

5000- 71

100 m/z A/ WA 6.20 6.40 71.05 6.60 6.80 55.02%

m/z-> ! • ' I G ■ |" | > 11 'I 20 25 1’’ 1TTT il TTTTTTTTT 111111 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 +-85 Abundance #63357: 3-Hexanone ' 43 57 1 , -AP — — 29 6.20 6.40 6.60 6.80 5000- 71 m/z 41.10 27.96% 100 85 | _______________________________ 1 ■______________________________________ J______________ ‘1’01110011117 1T‘ TTI"I‘‘T । ■ i ■ <| >< । i । i i i i ! i i i i । । i i i । ■ i i i । i i t i । >> r > t i i i i । i i । i । i I r i ! i i i i । i i

m/z-> Abundance 20 25 30 35 40 45

43 50 55 60 65 70 75 80 85 90 95 100 105 #1528: 3-Hexanone 57 6.20 AAAAA 6.40 6.60 6.80 m/Z 100.0 27.91% 29 71 5000 100

T....... I- m TDTTTTTTTTTT I ■" ' I " ’ ■ I TPTTUWTTTTTTTTT I"'1 r 85 1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27679.D NP112701.M Thu Dec 20 11:42:10 2001 Page 5

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