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GCMS analysis results for sample AD27678, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27678 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033247–000033262

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033256
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27678.D Vial: 5 Acq On : 19 Dec 2001 10:48 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.55 0.52 ng/uL 124593 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 entative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 90 3 2 - Hexanone 100 C6H120 000591-78-6 90 4 2-Hexanone 100 C6H120 000591-78-6 90 'Abundance 7 4 Scan 187 (6.554 min): 27678.D (-) m/z 43 • 10 100.00%

58 5000-

■ ' i"''1 ■ i ' ■ ' ■ । ■ i —Ir1f ■ ■ I.... I..................... ....... 71 85 100 6.20 6.40 6.60 6.80 7.00

m/z-> +..... 4 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ThpmmTT m/z 58.10 53.57% 'Abundance #63385: 2-Hexanone 43

5000- 58 .... La..... 6.20 6.40 6.60 6.80 7.00 29 /z 41.10 19.40% 39 71 85 100 1' I'1" I । i'' ■ ■ i1 ■ ■11 r'" i TT f Tp mPP m/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386:2-Hexanone 43 AAA, 6.20 6.40 6.60 6.80 7.00 5000- 58 m/z 57.10 15.11% 29 __________ ___________ r___________ Il________ 71 85 19° TTTpTTTpT-TTpTTTTTTTTpTTTTTrrTp^ Pmpmupun)—n]——/ 11'1 ’11 m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 43 #1556:2-Hexanone At AAA 6.20 6.40 6.60 6.80 7.00 TT

m/z 100.05 10.56% 58 5000 -

27 39 71 85 100 -H + ...... TTTTTT 11••" ।■11•। •11 > । r "' i I" " I m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

27678.D NP112701.M Thu Dec 20 11:41:08 2001 Page 2

NYC-WTC_000033256

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NYC-WTC_000033256Source: NYC Law Department, mirrored locally

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