GCMS analysis results for sample AD28166, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28165.D Vial: 15 Acq On : 22 Dec 2001 6:40 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

6.40 0.54 ng/uL 144005 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 entative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 86 2 3-Hexanone 100 C6H120 000589-38-8 72 3 3-Hexanone 100 C6H120 000589-38-8 56 4 3-He: none 100 C6H120 000589-38-8 56 Abundance Scan 170 (6.403 min): 28165.D (-) m/z 43.10 . 100.00% 43 57

71 5000 100 11 AT ■ —I TTTTTT 6.00 6.20 6.40 6.60 6.80 — ........ ,,53 85 —I—WNEPTTTTT m/z 57.1.0 88.53% I'''' I ‘1'' I " r ■" i miz-2 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57

5000 29 71

100 6.00 6.20 U 6.40 6.60 6.80 m/z 71.0.5 50.99%

miz-> " r ■" i TT TPPTTTTTTTTTT 111H " 111111 H 1" ' l1 ' T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63356: 3-Hexanone 29 43 57 — 4 . , I i I I I S 6.00 6.20 6.40 6.60 6.80 5000 71 m/z 100.1,5 31.72% 100

miz-2 " I " " I'11' I -38,+........ H....... dmmmmmmmmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357: 3-Hexanone ’ ’ ........‘ 43. 6.00 6.20 6.40 6.60 6.80 57 m/z 41.10 26.93% 29 5000 71

m/z~> "I""!1 mm tmmmmm H111"'' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 4s 6.00 6.20 6.40 6.60 6.80

28165.D NP112701.M Fri Dec 28 09:57:05 2001 Page 1

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