GCMS analysis results for sample AD27766, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27766.D Vial: 9 Acq On : 20 Dec 2001 3:13 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.59 1.66 ng/uL 496929 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2 -Hexanone 100 C6H120 000591-78-6 91 Abundance Scan 191 (6.591 min): 27766.D (-) m/ z 43.1.0 100.00% 43

58 5000-

391 7153 | 85 100 6.20 —MAA... 6.40 6.60 6.80 7.00

miz-> .............. #4 IPNHT TPPPTTTTT— 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 l' "' 1 TTT) m/ z 58.10 52.33% Abundance #63385: 2-Hexanone 43

5000 58 ......... 6.20 A- 6.40 6.60 6.80 7.00 29 m/z 41.05 16.60% 39 71 85 100 I " i ‘ " i1 ■ mIt Tmmj111

,—_NW miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556: 2-Hexanone 43

6.20 6.40 6.60 6.80 7.00 58 5000 - m/z 57.10 15.09%

27 39 71 85 100 1I I I" ' ’ 11 ” 'T T’’TTT I " " I'' ■' I ‘IT r miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384:2-Hexanone 43 6.20 6.40 6.60 6.80 7.00 m/z 100.05 10.19% 5000 - 58 29 39 100

m/z-> TTter TT+ 11" " r 71 ............... I 85 —— 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 r mm -------------- 6.20 6.40 6.60 6.80 7.00

27766.D NP112701.M Thu Dec 20 11:45:22 2001 Page 2

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