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GCMS analysis results for sample AD27623, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD27623 conducted on January 3, 2002.

NYC-WTC_000033082–000033096

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033090
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27623.D Vial: 14 Acq On : 20 Dec 2001 7:47 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.49 0.87 ng/uL 272360 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexangne. 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 91 4 3-Hexanone 100 C6H120 000589-38-8 78 Abundance / Scan 180 (6.489 min): 27623.D (-) m/z 43.10 100.00% 43 57 71 5000 100 A 6.20 6.40 6.60 6.80

m/z-> "' r " ' r 34 +] 85 t TIT । TTTTTTTT .............I" ’ ■ I ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/ Z !57.10 95.19% Abundance #63358: 3-Hexanone 43 57 —

71 — 5000 6.20 6.40 6.60 6.80 100 m/z 71.0.5 56.33% — 11U 85 I ‘' 111'11 ‘1'' I im Trm-| T . T TI" i n IT 11 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 43 57 29 Th 6.20 6.40 6.60 6.80 71 m/z 41.10 27.79%

JW 5000 100 85 I—0II—001——0000U0Tr TTTTTTTT r " ' r ■ " i11'' i TT +T r m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57 6.20 6.40 6.60 6.80 m/z 100.05 27.73% 29 71 5000 - 100

m/z-> . ... 111" I" TPH ■ i''" i" i' ■ ■' i " ■ ■ i TTn 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 + 6.20 6.40 6.60 6.80

27623.D NP112701.M Thu Dec 20 11:39:07 2001 Page 1

NYC-WTC_000033090

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NYC-WTC_000033090Source: NYC Law Department, mirrored locally

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