GCMS analysis results for sample AD27957, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27957.D Vial: 13 Acq On : 21 Dec 2001 3:06 am Operator: GALOS Sample : gems unknown 11/20 Inst ‘ : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.47 0.58 ng/uL 251050 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 72 4 3-Hexanone 100 C6H120 000589-38-8 59 ■Abundance Scan 177 (6.465 min): 27957.D (-) m/z 43.10 100.00% 43 57

71 5000 100 A m 20 25 30 35 40 ++ TTTDTT + ""I....... m/ z 39 6.20 ' 1 6 40 6 60 6.80 !57.10 91.89% m/z-> 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57

29 71 W. 5000 f" 6.20> 6.40 6.60 6.80 100 m/ z 71.05 52.81% 85 TITTTTTTTTTT TPTTTT TTTTITTTTT T TTTTTTTTTTT Wgunr....... — ■1-1-07 r miz- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358: 3-Hexanone 43 57 6.20 6.40 M 6.60 6.80 5000 71 m/z 100.15 30.24% 100

"IIUITuuir +T r11 • i mmm miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone / 43 6.20 6.40 6.60 6.80 57 m/ z 41.10 28.28% 29 5000 71

85 mm i' ”111111 r * TTppup i ■ ■ ■ ■ i ■ ■ ■ ■ i ■' ■ ■ i ■'' ‘ i ■ ■ ■ ■ TIUgTp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 _ NW TII ' ’ II’ 1111111111 TIT 6.20 6.40 6.60 6.80

27957.D NP112701.M Fri Dec 21 10:07:16 2001 Page 1

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