GCMS analysis results for sample AD27957, Jan 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC 1901\27957.D Vial: 13 Acq On : 21 Dec 2001 3:06 am Operator: GALOS Sample : gems unknown 11/20 Inst" : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.58 1.15 ng/uL 497825 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 _______ 000591-78-6 91 Abundance S Scan 189 (6.576 min): 27957.D (-) m/z 43.10 100.00% 43

58 5000 I A-A- 71 85 100 6.20 6.40 6.60 6.80 7.00 --- 53 | ’I.. THT |.|r,.,.|.Ir,TT — I""I — r m/ z 58.10 53.09% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556: 2-Hexanone 4b

5000 58 TTITTTTI 6.40 6.60 6.80 7.00 6.20 m/z 41.10 15.96%

_ m.. 27 71 85 100 5 —mmmmm 1DTTT ‘ I “ 1 qcin | i i । । । । । i TTT 11 | । i । i । m ‘T i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: 2-Hexanone 43 6.20 ' 6.40 ' ' 6.60 ' 6.80 " 7 00 5000 58 m/z 57.10 15.82% 29 71 85 100 m/z- Abundance ■ 11 |■i■i|iirif11111■t >11rI mmp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 43 #63385:2-Hexanone II"’ AW.. — 6.20 6.40 6.60 6.80 7.00 m/z 100.. 15 8.86% 5000 58 29 71 85 100 miz-> " I"m h............. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

27957.D NP112701.M Fri Dec 21 10:07:18 2001 Page 2

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