GCMS analysis results for sample AD27957, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27957.D Vial: 13 Acq On : 21 Dec 2001 3:06 am Operator: GALOS Sample : gems unknown 11/20 Inst * : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.47 ng/uL 202582 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexano 102 C6H14O 000623-37-0 83 2 3-Hexa: 1 102 C6H140 000623-37-0 83 3 3-Hex iol 102 C6H140 000623-37-0 83 4 3-He: nol 102 C6H140 _____ 000623-37-0 83 Abundance Scan 203 (6.704 min): 27957.D (-) m/z 59.10 100.00% 59 55

5000 73 43 -A ----------------- 39 6.40 6.60 6.80 7.00 mmmm +4 NTTTTTTTTTTUTTTTTTTTTTTTTTTTTTT m/z 55.10 79.20% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol 59 55

5000 31 i k I 1... I ll III I I i I l i i i i I 73 27 6.40 6.60 6.80 7.00 m/ z 73.05 41.18% 102 TTTTTTTTTTT I............ -n-rr.jm rp —‘1’11’1 tt rrrr. TTT ‘ T miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531:3-Hexanol 1 59 55 . I ' ■ i ■ ■ ■ ■ i ■ ' ■ ' i ' ■ ■ ■ i ■ ■ • * i 6.40 6.60 6.80 7.00 5000 73 m/z 43.10 30.20% 43 39 ! 69 . ‘' 111" P1" i " " I'"1 p H1 i111111"1 p " ■ P " ■ i" ■ ■ r ■ TTTUpp] —....... miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762: 3-Hexanol 55 59 6.40 6.60 6.80 7.00 m/z 41.05 24.21% 31 5000 27 43 73

_________________ 102 11 11"1 I...... . . ।.... p ... ।.... ।... q 1.1,111 <<. 11... 11. ■ ■ r1 ' ■ ■ ' I ' ' ' ' I ' ' ' ' I ' ' ' T I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27957.D NP112701.M Fri Dec 21 10:07:20 2001 Page 3

NYC-WTC_000034148