GCMS analysis results for sample AD27957, Jan 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC19 01\27957.D Vial: 13 Acq On : 21 Dec 2001 3:06 am Operator: GALOS Sample : gems unknown 11/20 Inst * : GC/MS Ins Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.69 ng/uL 297433 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 78 3 2-Hexanol, (R) - 102 C6H140 026549-24-6 64 4 2-HeKanol 102 C6H140 _________ 000626-93-7 64 Abundance Scan 215 (6.814 min): 27957.D (-) m/z 45.10 100.00% 45

5000

---IPP >i,i — 41 . 69 5356 I 6.40 6.60 6.80 7.00 7.20 i miz-> .................. 38 14 •.......... Ip 84 87 1 m/ z +TTTTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 TTTTT-rp-rrtIWTp 41.05 13.36% Abundance #63584:2-Hexanol

5000 45

69 MU 6.40 m/z 6.60 69.10 6.80 7.00 **ffr 7.20 13.26% 56 miz-> —. 19—. 27,31.... 424 WTT 1 84 87 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 TIWWI1WTITTTITTTTTT

Abundance " #63546; 2-Pentanol. 4-methyl- 45 TTTTIIPTTTTT 6.40 6.60 6.80 7.00 7.20 5000 m/ Z 43.10 11.40% 27 69 19 42 31 57 84 87 TTTTTTTTTTNTTTTT 1111 m।.... ।. 1, 111. (, ।., I" " I " ” i u " ib ■■ ■ i ■■ ■' i " " i miz-> 10 15 20 253035 40 45 50 55 60 65 70 75 80 85 90 95 Abundance» j ...... ~ #1794: 2-Hexanol, (R)- t-n T’rrrrT 45 6.40 6.60 6.80 7.00 7.20 m/z 44.10 8.86% 5000

i |• . -9-H29 39 42 55 TTTTTTI TIWIPIWTTITT __________ 84 87 69 | ‘ ‘ | ' 1 1 q1 n I p ) I I | 11 I I | 11 A I AA AA miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27957.D NP112701.M Fri Dec 21 10:07:22 2001 Page 4

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