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GCMS unknowns analysis results for sample AD27872, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD27872 conducted on January 2, 2002.

NYC-WTC_000034018–000034031

Folder label: “GCMS X 11/20/01 A 12/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27872 .D Vial: 4 Acq On : 20 Dec 2001 6:53 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.83 ng/uL 281963 1,4-Dichlorobenzene-d4 11.86

Hit# Of 5 /■tentative ID MW MolForm CAS# Qual 1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Hexanol 102 C6H140 000626-93-7 83 4 2-Pentanol, 4-methyl- 102 C6H140 _______ 000108-11-2 74 Abundance Scan 215 (6.813 mln): 27872.D (-) m/z 45.10 100.00% 45

5000

m.. 41 „ 69 84 87 + ... 535859..... 1..... - — . ।। . 6.40 6.60 6.80 7.00 " 7.20 m/z 41.10 14.96%

JW miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance> #63582: 2-Hexanol 45

5000 I • ■ t ‘ I ‘ ■ I • 6.40 6.60 16.80 7.00 7.20 27 69 m/z 69. 12.77% 19 31 42 57 84 87 TWTTIIDTI l1" ' I' TIP TITITTTHHTTTTTTTTT 11TT1111 ‘ TTUTmgn miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 45

6.40 6.60 6.80 7.00 7.20 5000 m/ z 43.10 11.72%

69 19 27 31 42-! 56 84 87 T t..... T’T T TIUTTTTTTTTTT A i • • ’' i" TrrTTT miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583:2-Hexanol TIITrrTTTrr—rrur— 45 6.60 6.80 7.00 7.20 6.40 m/z 44.1.0 9.75% 5000 -

69 27 31 3942 Iur . , j . . . q , . . i | , ; , , | l . rTITH 555g | TTHHTPT TTI—TTTTTTTTTTT’ 84 87 AAA AaA/Lans 4 4 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27872.D NP112701.M Fri Dec 21 09:56:55 2001 Page 4

NYC-WTC_000034029

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NYC-WTC_000034029Source: NYC Law Department, mirrored locally

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