GCMS unknowns analysis results for sample AD27872, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27872.D Vial: 4 Acq On : 20 Dec 2001 6:53 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.69 0.57 ng/uL 193876 1,4-Dichlorobenzene-d4 11.86

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hex-- anol ■Abundance Scan 202 (6.694 min): 27872.D (-) 102 C6H140 000623-37-0 83 m/z 59.10 100.00% 55 59

5000

39 43 73 . AL. 6.40 6.60 6.80 7.00 mp ----- ■ 11 “ 41 ......mr TIWWTTTTTTTTTTOTTITT m/z 55.10 83.72% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527:3-Hexanol — 59 55 - 5000 73 31 6.40 6.60 6.80 7.00 m/z 73.05 42.16% .4 27 TTTTTTTTTTT .. 4 t TTmTTuOTTTr 84 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol 59 55 ' ....... \.... - 6.40 6.60 6.80 7.00 73 5000 - 31 m/z 43.10 31.83% 27 : 45 84 “r ••• “i TIWTTTTTTTTETTTTTTTTTTNTDTTTTTTTTTT IT I" u l T — m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol . TT.. 1. 1.. 1-T-r-

! 55 59 6.40 6.60 16.80 7.00 m/z 41.10| 24.94% 31 5000

, JW _ 27 43 73

102 TTITTI—r TTT 11''" I......... H ‘I‘T‘01111—0000170TTTTTTTTT m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 6.40 6.60 6.80 7.00

27872.D NP112701.M Fri Dec 21 09:56:54 2001 Page 3

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