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GCMS unknowns analysis results for sample AD27872, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD27872 conducted on January 2, 2002.

NYC-WTC_000034018–000034031

Folder label: “GCMS X 11/20/01 A 12/20/01

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Scanned page image, NYC-WTC_000034027
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1 901\27872.D Vial: 4 Acq On : 20 Dec 2001 6:53 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.57 1.33 ng/uL 455109 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 / Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 _______ 000591-78-6 91 Abundance........... Scan 188 (6.565 min): 27872.D (-) m/z 43.1.0 100.00%! 43

58 5000

Tdr ------- 391 • ।' ] > < । > I > • > 111 > ■> 11111111 50 71 85 100 6.20 6.40 6.60 6.80 7.00 Ip] +TTTTTTTTTTTTTTTTTTTTTT’’I’’’II mT|T-i-rrp m/ z 58.1,0 52.43% miz-2 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386: 2-Hexanone 43 — 5000 58 6.20 6.40 6.60 6.80 7.00 29 m/z 57.10 14.76% 71 85 100

mz-> 1 “| H U| 1 .......... । Tmt 1TTTTTTTTTTTTTTTmTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance, #63385: 2-Hexanone — 43 PrTr HA i-i . 6.20 6.40 6.60 6.80 7.00 5000 58 m/z 41.10 14.55%|

JU 29 39 71 85 100 TmTTTTTTTmTmTP m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384: 2-Hexanone..... ■ • i ■ ■ • 1 l • ' 1 1 I ' PM1 43 6.20 6.40 6.60 6.80 7.00 m/z 100. .15 9.13 5000- 58 29 71 mRmmmmn85 39 100 —.... N \ . ...... miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

27872.D NP112701.M Fri Dec 21 09:56:52 2001 Page 2

NYC-WTC_000034027

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NYC-WTC_000034027Source: NYC Law Department, mirrored locally

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