GCMS analysis results for sample AD27623, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27623.D Vial: 14 Acq On : 20 Dec 2001 7:47 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.84 1.12 ng/uL 351384 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Hexanol 102 C6H140 000626-93-7 83 4 2-Pentanol, 4-methyl-_____________ 102 C6H140 000108-11-2 74 Abundance — Scan 218 (6.838 min): 27623.D (-) m/ z 45.10 100.00% 45

5000 ——V 41 69 । ‘ 111 6.40 6.60 6.80 7.00 7.20 34 44 84 87 53 *6 59. ■ 111 TIrr1 mpm m/ Z 69.10 15.65% m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583: 2-Hexanol 4)5

-------------\ 5000 - 6.40 6.60 6.80 7.00 7.20 m/ Z 41.10 14.88%

J 69 ... -2,31 mH 39 42, |1 ■58 ■ i ■ • • ■55 >•i■• ■■। ■ |11 ■ 84 87 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 45

6.40 6.60 6.80 7.00 7.20 5000 m/z 43.10 13.15%

69 .. 19..27, 31. 42, ' 111'11''1 ’ I ‘’111 56 1]WIII]PIuupgoTn ! 84 87 m/z-> Abundance 10 15 20 25 30 35 40 45

45 50 55 #1792: 2-Hexanol 60 65 70 75 80 85 90 95 , AAA A....... — 6.40 6.60 6.80 7.00 7.20 m/z 44.05 9.56% 5000

69 a 4 AAA m/z-> 10 ......... 7731... 3942. 15 20 25 30 35 40 45 TTTT 50 55 58 mH 55 60 — 65 70 75 80 84 87 > i • • • ■ i • > ■»।■ i ’ ’ ■11 ■ 85 90 95 6.40 6.60 IAAAPMA4 6.80 7.00 7.20

27623.D NP112701.M Thu Dec 20 11:39:13 2001 Page 4

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