GCMS analysis results for sample AD27766, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27766.D Vial: 9 Acq On : 20 Dec ’2001 3:13 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) . Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6

R.T. EstConc Area . Relative to ISTD R.T.

6.49 0.92 ng/uL 275803 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 86 4 3-Hexanone 100 C6H120 000589-38-8 72 Abundance Scan 180 (6.490 min): 27766.D (-) m/z 57.10 100.00% 43 57 71 5000 100 ===== . ......................... 6.20 6.40 6.60 6.80

m/z~> -1 +53+ 85 ...... TIT ri 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 "I............. m/z 43.10 99.26% Abundance #63358:3-Hexanone 43 57

5000 71 100 - —AA6.20 6.40 6.60 6.80 m/z 71.05 59.42% 85 I ' • < ‘ f • •'»| ’ TTTTTT +T I •' " I •'" I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

A Abundance #63357:3-Hexanone 43 57 29 6.20 6.40 6.60 6.80 5000 71 m/z 100.15 . 28.79% 100 I I 85 I’■■■I■'''I•''' I'''' I I I m |.. r, 11 n r| i' *11111" i'111 r1 ’1111111 r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone Tr/ - 43 57 6.20 6.40 6.60 6.80 m/ Z 41.10 27.76%

m/z-> 5000- 29

TTTTTT 1"1' 1111' I' l TITTTTTTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 71

+85 100 ... W 6.20 6.40 6.60 6.80

27766.D NP112701.M Thu Dec 20 11:45:20 2001 Page 1

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