GCMS analysis results for sample AD27628, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27628.D Vial: 18 Acq On : 20 Dec.2001 1:24 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) k

Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.44 1.26 ng/uL 298460 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 87 3 3-Hexanone 100 C6H120 000589-38-8 64 4 3-Hexanone 100 C6H120 000589-38-8 56 Abundance Scan 174 (6.436 min): 27628.D (-) m/z 43.10 100.00% 43 57

71 5000 100 Tddnnrn TTT 39 6.20 6.40 6.60 6.80 6.00 53, 85 - 4 WTpTf TTI] I" '' I r m/z 57.10 95.18% mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #1528: 3-Hexanone __ Abundance 43 57

29 71 5000 —TT1 6.00 6.20 6.40 6.60 6.80 100 m/ z 71.05 51.18% 85 . T.. 1 ...... I1 i""l'

U ■11 ‘ '111 i" " i i ‘ " I' m/z->20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57 i ' ■ ■ ' I - 6.00 6.20 6.40 6.60 6.80 71 m/z 100.15 28.37% 5000 100

85 r''' i' ■' ■ r ' ■' i TTT TPIpBpBBnn i •■ ■ ■ i r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 43 6.00 6.20 6.40 6.60 6.80 57 m/z 41.10. 26.80% 29

m/z-> 5000

TT 71

T 1111" I...... T TI—Trr i" " i TTI0‘E"‘1"—UTTEEETTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 85 100

' r " ’ r 6.00 6.20 MW 6.40 6.60 6.80

27628.D NP112701.M Fri Dec 21 09:19:12 2001 Page 3

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