GCMS analysis results for sample AD27628, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27628.D Vial: 18 Acq On : 20 Dec 2001 1:24 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1-Butanol Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

5.14 0.56 ng/uL 131747 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H10O 000071-36-3 28 2 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 9 3 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 9

5 4 Oxirane, ethyl- 72 C4H80 000106-88-7 9 'Abundance Scan 33 (5.143 min): 27628.D (-) 4 56 59

5000

49 71 77 5.00 5.20 5.40 5.60 45 —— ’II + j I ■ ■ ■ 11'1'' i " " r " ' i ■ ■" i • ■ " I' ' I' ’ ■ 'I* —- m/z 43.10 82.16% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 'Abundance #62584: 1-Butanol 41 56

5000 . 111 Tr 5.00 5.20 5.40 5.60 m/z 5 .10 79.81% 45 3^i 53 I‘‘‘-111‘‘1—11-T"IIITT ■ > ■ i >. •. । . 111 ■ TTttT ,||||||(TT miz--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63578: 1 -Pentanol. 4-methyl- 56 41 69 5.00 5.20 5.40 5.60 5000 m/z 59.10 67.99%

m/z-> Abundance 5

5000- 10 15 20 25 30 35 4s.m 60 65 70 40 45 50 55 #1787: 1 -Pentanol, 4-methyl-

41 159

56 ‘ i ‘‘‘IT rrTTp-TTTp-rrr , . . . . । . . . . ।

69 75 80 85 90 84 .

_N_ 5.00 m/z 42.10 5.20 5.40 5.60 65.16%

27 31

15

m/z-> i''' ■ i 458 ——— 84 1IWmuuutu—nnpr 45 ■ । ■ ■ • • ।11" । ■ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ' I'' ‘' I 1—। 5.00 5.20 5.40 5.60

27628.D NP112701.M Fri Dec 21 09:19:10 2001 Page 2

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