GCMS analysis results for sample AD27764, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27764.D Vial: 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1-Butanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.12 2.46 ng/uL 623955 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol / 74 C4H10O 000071-36-3 38 2 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 33 3 l-Hexene/ 84 C6H12 000592-41-6 33 4 Pentanal , 3-methyl- 100 C6H120 015877-57-3 32 Abundance Scan 31 (5.124 min): 27764.D (-) m/z 41.10 100.00% 41 56

5000 fTTTTyTT UII—CTuOT 45 71 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z-> 20 25 30 374 +51 + 30 67 | l| I I I I | M l I | I I I I |

35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 I'1 " f''1111 " ' i111' i'1 m/ z 56.10 73.93% Abundance #62584: 1-Butanol 41 56

5000 TT IT TT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 59.10 67.43% 45

m/z-> '' r p-rr 37 +— Tp-r —PP—MT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 । ।। r. . . । ।।।।।

Abundance #63578: 1-Pentanol, 4-methyl- 56 41 I"nI''"I""I"'j’ 69 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- 1 m/ Z 42 .,10 65.30%

45 | 60 84 i11" i 11' 1 ■ ■ r '' ■ r TTTTTTTTTTT 11 ‘1' 1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62755: 1-Hexene 41 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 m/ z 43.10 62.03% 5000 -

AW 84 69

'' I "' • IB Trmmupurt —514 Pw]ur p-n 11 111 r|Tr 11 > > 11 .11.11।. ।. 11. । r 11 ‘i1111111'' i111 ■ i TTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

27764.D NP112701.M Thu Dec 20 11:43:22 2001 Page 2

NYC-WTC_000033295