GCMS analysis results for sample AD26626, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Butanol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

5.10 1.12 ng/uL 344175 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H10O 000071-36-3 38 2 Pentanal, 3-methyl- 100 C6H120 015877-57-3 38 3 1-Hexene 84 C6H12 000592-41-6 33 4 1-P tanol, 4-methyl- 102 C6H140 000626-89-1 33 Abundance Scan 29 (5.105 min): 26626.D (-) m/z 41 10 100.00%| 41 ii 56

5000-

---34 +514 + 45 71 3 1′1′11′1111111 TWPuumpTT TTTT । 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z-> 67 100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 i ’ * • H " 1 r ' *' i '' I' " ' I m/z 56 10 78.28% Abundance #62584: 1-Butanol i 41 56

— r,.... 1 5000 TTPTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59 10 69.76% 45 37 ,1 TTTTTTTTTTT p-rr 1 i ""I" TTT’TTTTTTTTTTTTTTTTT m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63404: Pentanal,.3-methyl- 56 TOT T . -I - pT . , j . , , II 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z 42 05 66.98%

J 27 44 71 i• 1 67 | 82 100 ■ ।1"11 ’ ’ITTTTTETTTTETTTTTTTTTT I"1 ■i T"‘TITTTTT TVVTNur 1111 > 11 ■ ■ i'" ■ i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #62755: 1-Hexene '1 111 (11'1 ’ Tr PnT 41 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 m/z 43.05 56.13% 5000- 84 69

" r "1 r "I""!"1 —14 TIIWWNOHgu TTETIETTT’TTITCITTTTT m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26626.D NP112701.M Fri Dec 07 14:49:59 2001 Page 2

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