GCMS analysis results for sample AD26315, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV30 01\26315.D vial: 24 Acq On 1 Dec 2001 9:07 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Butanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 5.21 0.50 ng/uL 140764 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 entative ID MW MolForm CAS# Qual 1 1-Butanol, 74 C4H10O 000071-36-3 17 2 Guanidi: 59 CH5N3 000113-00-8 9 3 Cyclobu ane 56 C4H8 000287-23-0 9 4 1-Pentanol, 4-methyl - 102 C6H140 000626-89-1 9 Abundance Scan 40 (5.206 min): 26315.D (-) m/z 41.10 100.00% 41 56 59 5000 71 45 ' 5.00 1520 — 5.40'15.60 1 miz-> 34 — +T—dt—67 Tam ‘' 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 m/z 56.10 70.76% Abundance #62584: 1-Butanol

AN 41 56

5000 ■ ■ i ■ • • • i 1 ■ 5.00 5.20 5.40 5.60 m/z 59.05 69.38% 45

miz-> 10 15 20 25 30 — 3l n... . 35 40 45 50 55 60 55 70 75 80 । ■' i ■ ■' • i ■ ■ • ■ i ■ ■ ■ • i ■ ■ ■ ■ i

Abundance #100: Guanidine 43 59 ■ • i — 5.00 5.20 5.40 5.60 5000 m/z 43.05 65.14%

17 ---- 27 31 -40 TTp-rTTTTTTTTT A T| i i i < j i i i i । i i ! 1 i “ 11 ' 11 I I■ " ‘ ‘ 11 '' miz—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62310: Cyclobutane 1/1ttm II , . , Tdl18.7 • । ' 41 5.00 5.20 5.40 5.60 56 m/z 42.05 54.80% 5000 27

38 49 33 m/z—> 11011 1’0110 ’ 11 TIT ■ Hl l -H — ——— TTTII 10 15 20 25 30 35404550556055 70 75 80 AA/W 5.00 5.20 5.40 5.60

26315.D NP112701.M Tue Dec 04 10:11:44 2001 Page 2

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