GCMS results log, sample AD26982, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26982.D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Pentanol, 4-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.16 0.83 ng/uL 344128 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Pentanol/ 4-methyl- 102 C6H140 000626-89-1 28 2 1-Butanoy 74 C4H10O 000071-36-3 25 3 Guanidine 59 CH5N3 000113-00-8 9 4 Cyclobucane 56 C4H8 000287-23-0 9 Abundance 7 Scan 34 (5.156 min): 26982.D (-) m/z 41.10 100.00% 41 56 59

5000 TInTT 45 71 67 1 5.00 5.20 5.40 5.60

I m/z-> 10 15 20 25 30 35 3440 45 5053 50 55 60 65 70 75 TT TTTTTTT ' I' " ' I'' " I' 80 85 90 m/ z 84.74% Abundance #63578: 1-Pentanol, 4-methyl- I

41 56 69 5000 5.00 5.20 5.40 5.60 m/z 59.10 75.35%

m/z-> r,. r< .| n । 10 15 20 r। 25 30 । 35 ।. 40 4 | 59 ' " I " ' ■ T' 45 50 55 60 65 TTTuim 84 70 75 80 85 90 'Abundance #62584: 1-Butanol 41 56

5.00 5.20 5.40 5.60 5000 m/z 43.05 69.72%

m/z-> Abundance 38 45 53. TI]Pn]unum)mTv I . . , . I I > | . . . < t .... | 10 15 20 25 30 35 40 45 50 55 60 #100: Guanidine 43 59 65 । । 70 । 75 80 । । 85 । . 90 —N5.00 m/z 5.20 42.05 5.40 65.69% 5.60

'm/z-: 5000

17 1' 11' ” I'1'' 11 10 15 20 27 31 --+--49 25 . 30 35 40 T-p-rrrp-rTTT-rrr 11" ' i" " I ■' ■ ■ r " ■ i • ■ " i'' ■b i ■ ■ 45 50 55 60 65 70 75 80 85 90 J 5.00 5.20 5.40 5.60

26982.D NP112701.M Tue Dec 11 14:48:45 2001 Page 2

NYC-WTC_000032352