GCMS results log, sample AD26982, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26982.D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.53 ng/uL 220909 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 MW MolForm CAS# Qual

1 Cyclohexane, thyl- 98 C7H14 000108-87-2 97 2 Cyclohexane,methyl - 98 C7H14 000108-87-2 95 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 91 4 Cyclohex e, methyl- 98 C7H14 000108-87-2 60 Abundance Scan 22 (5.046 min): 26982. D (-) m/ z 55.10 100.00% 55 S3 I

5000 41 98 69 .. J I• ' ’' I T I 4.90 5.00 5.10 5.20 5.30 5.40 5.50 51 ,, •i ■ ■ i• HT TH —544— ' i ’ • ■ ■ i1 77 11111 ■ । ■1 PTTT + m/ Z 83.05 94.94% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83 i 98 ।....।.iij।,<i.।.. .,। .J 5000 T 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 47.80% 66 I! TTT l'' TTT yn rq-r ■ i ■" ■ i ■ TIT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- — □□ 83 T‘EETTETTTT‘‘‘‘I‘‘L‘T 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z ,98.05 42.62% 42 27 69

■ । ■ ■' ■ ।1 ■ ■11 ■ ■ ■ ■ ।।' ■ ■ ■ । ■ ■ ■ ■ । ■ TT I ’1 ” I ‘I‘"E‘1-TTTTE"‘It‘EII‘SEII‘ICTTTTTITTT m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63235: Cyclohexane, methyl- 55 83 p rrr । + ■p-rr-rr I' •'' I' • 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 56.10

_N_ 31.68% 5000 98 42 69 27 I m/z-> ’ 11 TT prm-j- i" ■' । i-rq-r ..... HI.......... i I ‘ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ‘ I • i" " i" + —OOTuuuuuumnuuuur 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26982 .D NP112701.M Tue Dec 11 14:48:43 2001 Page 1

NYC-WTC_000032351