GCMS results log, sample AD26346, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26846.D Vial: 30 Acq On 7 Dec 2001 1:30 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.49 ng/uL 212695 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 3 Cyclohexane, methyl - 98 C7H14 000108-87-2 95 4 Cyclohexane, methyl - 98 C7H14 000108-87-2 78 Abundance Scan 23 (5.050 min): 26846.D (-) m/z 55.10 100.00% 55 88 41 5000 98

... ... 69 7' Are i' ■ ■ ■ i 4.90 5.00 5.10 5.20 5.30 5.40 5.50 — +504 - TT m/ Z 83.05 98.62% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83

98 — 5000 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/ Z 60.48% 661 41. 10 • । i" • । ■ ■ • ■ । ■ 11 ‘' I" " I'' ITTer Pp m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- 55 83 LA i' ■ • ■i " ■' i' ■' ■ i 4.90 5.00 5.10 5.20 5.30 5.40 5.50 TT

5000 98 m/z 98.15 48.48% 42 27 69

TI]PP1TTTTT]n]W]nm]m]uuuuauuuwT"guT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- - I'1'' I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 42.10 34.32% 5000- 98

A 42 69 27

m/z-> - 11" 11 +TTTT — TT’Trr -H 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 MA "TT’TTTTTTTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26846.D NP112701.M Tue Dec 11 14:47:47 2001 Page 1

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