GCMS Analysis Report for Sample AD26336, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26336.D Vial: 30 Acq On : 1 Dec 2001 2:36 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 4.96 0.48 ng/uL 152004 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 4 Cyclohexane, methyl- 98 C7H14 000108-87-2 78 Abundance Scan 13 (4.958 min): 26336.D(-) 55 83 m/z 83.05 100.00%|

41 5000 98

69 TMummr 4.90 5.00 5.10 5.20 5.30 5.40 H m +94. Imnpm m/z 36 51, mz-> TIPMTTTT H 20 25 3035404550556065 70 75 80859095 100 105 55.10 89.94% Abundance #63235: Cyclohexane, methyl- _ 55 3

5000 42 98 4.90 5.00 5.10 5.20 5.30 5.40 1

M. 69 m/z 41.05 53.45% 27 mmmmm PTpe mHmmp Tmppn 11" ■ ■ i1' ■ ■ mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- 83 55 4.90 5.00 5.10 5.20 5.30 5.40 5000 98 m/z 98.05 44.56% 42 27 69

miz-> ■‘i"" i ‘ •■ i i ■ ■ “ i ‘ “ i ‘ ' i" “ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 - m IT Abundance #63236: Cyclohexane, methyl- i" • ■ । “ “ i T i • * • ■ i 55 93 4.90 5.00 5.10 5.20 5.30 5.40

_As m/z 42.10 32.14% 5000 98 42 27 70

m/z—> +fll 119’11117 ■11 ■ ■ ■ • i “ ■ • i' 1 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 111’1117 p 4.90 5.00 5.10 5.20 5.30 5.40

26336.D NP112701.M Tue Dec 04 15:07:48 2001 Page 1

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