GCMS calibration table for method 208, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\NOV3001\26252.D Vial: 18 Acq On : 1 Dec 2001 3:40 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.46 ng/uL 219314 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 94 4 Cyclohexane, methyl-______________ 98 C7H14 000108-87-2 72 Abundance 7 Scan 19 (5.012 min): 26252. D (-) m/z 83.05 100.00% 1 55 83 41 5000 98 69 i11 ■ ■ i ■1 ■ ■ i ■ ‘1 • i ■(1 ■ i1" ■ i1 ■111 4.90 5.00 5.10 5.20 5.30 5.40 51, ,1 > 1 [ > 111 f i in t TOTTITTmgm 79 , 94 TITagua m/z . 55.10 84.54% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 55 83

5000 98 42 4.90 5.00 5.10 5.20 5.30 5.40 ' 69 m/z 41.10 50.87% 27 mmmmm m ■ m ' m I m m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

5000 #63236: Cyclohexane, methyl- 55 83

98 JU... 4.90 5.00 5.10 5.20 5.30 5.40 m/z 98.05 41.98% 42 27 70

■nfz-> ■ • i ■11 ■ i ■ ; i j. i.11. • ।. 11 111’1111111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I. fl —mmp 1 r" i' ■" Abundance #1326: Cyclohexane, methyl- —।— 83 4.90 5.00 5.10 5.20 5.30 5.40 55 m/z 43.00 38.07%

m/z—> 5000

- — 1111111 - 27 42

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 H 69

m 98

1 [i 11111111111 H JW T I“ 1 ‘ i ’ ‘ ' I “ ' ' I ‘ ‘ ‘'! 4.90 5.00 5.10 5.20 5.30 5.40

26252.D NP112701.M Tue Dec 04 10:11:04 2001 Page 1

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