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GCMS analysis results for sample AD26252, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD26252 with unidentified compounds detected.

NYC-WTC_000031236–000031247

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26253.D Vial: 32 Acq On 1 Dec 2001 4:25 pm Operator: GALOS Sample gc/ms unknown 11/3 +26319 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

5.00 0.55 ng/uL 178187 1,4-Dichlorobenzene-d4 11.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 93 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 90 4 Cyclohexane, methyl - 98 C7H14 000108-87-2 64 Abundance Scan 18 (5.004 min): 26253.D (-) m/z 83.05 100.00% 55 83

5000 41 98 — . 11 < < । < 11»111. । (< ।«11

69 4.90 5.00 5.10 5.20 5.30 5.40 ---36, + - ■ l - Hl ■ m ' H H m/z 55.10 91.77% mz-> 20 25 30 35 40 45 #63236:

J 50 55 60 65 70 75 80 85 90 95 100 105 Abundance Cyclohexane, methy- 55 83

5000 98 TPPAmm 42 4.90 5.00 5.10 5.20 5.30 5.40 27 70 m/z 41.10 48.10% +). n ।. 11 > 1111_ <. 11. i < 66 i • J • 1111 (i n 111—

U _ _ I, nil pin 11 < > «-p . •«............ th . .. ।। < 111 ।. 111 j > 11 11 11 +yu। i । 11 ! »j । Ij miz-> 20253035 40 4550556065 70 75 80859095 100 105 Abundance #1326: Cyclohexane, methyl- 55 83 IWImgPuuun 4.90 5.00 5.10 5.20 5.30 5.40 5000 98 m/z 98.05 45.57% 42 27 69

T TT1 " I'''' I " '11 ‘ -pr mmmm Imp Tp-rrrp-m miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- T i “' ■ i1 ■ ■11 55 a 4.90 5.00 5.10 5.20 5.30 5.40 m/z 43.00 35.71% 5000

■nfz-> 27 42

mmmm m rj 11 n Th 111:1111111 1111. < >. । > 11 mmmmRmmT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 69 |, 98

W 4.90 5.00 5.10 5.20 5.30 5.40 ‘ ‘

26253.D NP112701.M Tue Dec 04 10:11:22 2001 Page 1

NYC-WTC_000031244

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NYC-WTC_000031244Source: NYC Law Department, mirrored locally

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