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GCMS Analysis Report for Sample AD26387, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26387 with a note regarding unknown compounds.

NYC-WTC_000031433–000031451

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26387.D Vial: 13 Acq On : 30 Nov 2001 11:08 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.05 0.55 ng/uL 265236 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 81 2 Cyclohexane/ methyl- 98 C7H14 000108-87-2 72 3 Cyclohexanes, methyl- 98 C7H14 000108-87-2 59 4 2-Pentene, 4,4-dimethyl-, (E) -____ 98 C7H14 000690-08-4 53 Abundance Scan 23 (5.049 min): 26387.D(-) m/z ,83.05 100.00% r 55 83

5000 41 98

69 I•“•i“•‘i • i' " ‘ I ■' “ i " “ i' ■ 4.90 5.00 5.10 5.20 5.30 5.40 5.50

mlz-> 1’1’91115121101111117 11 -51+ mH ’ I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 DUpa # m/z 55.10 83.13% Abundance #63236: Cyclohexane, methyl- 55 83

5000 98 A4 11 ’ ’I 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/z 98.05 43.96% . 661 ... 111 •1 ■111 " I ■ • ■11" ■' I' 1’1111111117 H |-r 11 > । >-| 11 (i > > > 11 ■ 1111 i i > > *11 • * • ■ i ■ ■ 111 ‘ " I “ " mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63234: Cyclohexane, methyl- 55 83 T 11 ‘1 ■ ’ i “ ■' 11" ‘ i “ ■ ■ i “ “ i “ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z 41.05 41.22% 42 98 69 27 I “1 H - ! !■■■■!■■ "I T TTT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- TTTp-r TTTTTTT 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/z 56.10 25.14% 5000 98 42 69 27 11! " " I ‘ 1’1’1111111 '■'11‘'111 tpmmgt —mm —II——1T ■rrrpr nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26387.D NP112701.M Tue Dec 04 10:39:11 2001 Page 1

NYC-WTC_000031441

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