GCMS Analysis Report for Sample AD26387, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3 001\26387.D Vial: 13 Acq On : 30 Nov 2001 11:08 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Butanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.15 1.35 ng/uL 655127 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Butanol/ 74 C4H10O 000071-36-3 32 2 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 25 3 1-Hexene 84 C6H12 000592-41-6 25 4 Oxirane, (1-methylethyl)- 86 C5H10O 001438-14-8 16 Abundance Scan 34 (5.150 min): 26387.D (-) m/z 41.05 100.00% 41 56

5000

71 T TI ■

m/z-> " I'' “ 1‘' “ 1" " 1'1' 37 | 50 TpH 60 T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 L 100 । i>111 >111 ii111111111 n 11111111>11 5.00 m/ z 5.20 56.10 5.40 80.70% 5.60

Abundance #62584:1-Butanol 41 56

5000 IIIIT 5.00 5.20 5.40 5.60 m/z !59.10 77.68% 45 TIL—I—pampurf mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63578:1-Pentanol, 4-methyl- 56 41 69 5.00 5.20 5.40 5.60 5000 m/z 42.10 67.15%

m/z-> • '11' ‘ 'i 60 fl 84 TITT 1 ■'. * i1 * * ■ i1'11«‘ ■ i •»‘ • i * ‘ • • i •»■' I *" • 1 i1 “111 ■" i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62753:1-Haxene 1 • l • 1 • • i 1 • 41 5.00 5.20 5.40 5.60 m/z 43.10 62.37% 5000

AWN 27 84 69

mlz~> m p TIUIITH 111011111117 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Tu—nan 5.00 5.20 5.40 5.60

26387.D NP112701.M Tue Dec 04 10:39:12 2001 Page 2

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