GCMS analysis report for sample AD26393, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26393 .D Vial: 3 Acq On : 30 Nov 2001 2:02 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Butanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 5.12 1.07 ng/uL 461842 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Buta: 1 74 C4H10O 000071-36-3 38 2 1-Pen nol, 4-methyl- 102 C6H140 000626-89-1 25 3 Oxiri e, (1 -methylethyl) - 86 C5H10O 001438-14-8 12 4 Gua: dine 59 CH5N3 000113-00-8 9 Abundance Scan 30 (5.119 min): 26393.D (-) m/z 41 .05 100.00% 41 56 59

5000

71 45 4.905.005.105.205.305.405.50 38 1 .1 50 53 ।—67 m/z 56.10 86.06% —TTOOTTI ■ i ■ ■ ■ ■ i ■ “ 1111M 11 ■ ‘ ■ i miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62584: 1-Butanol 41 56

5000 = = m mem । L 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59 10 80.82% 45

miz-> I..,20..... ..... 344 25 30 35 40 d- 53 111] । 50 556065 70 75 80859095 । > TIUTT TT m p-m-y

Abundance #63578:1-Pentanol, 4-methyl- 56 41 In ‘11 ‘‘1’11113 4.905.00 5.10 5.20 5.30 5.40 5.50 69 5000 m/z.. 43.05 68.98%

45— 59 84 miz-> Abundance 20 —’61+106.10/11--TTTTS-I1 25 30 35 a" 40 45 50 55 60 ■1111'11' ■ Ouauum T!tf T-pau 65 70 75 80 85 90 95 ___________ #721: Oxirane, (1 -methylethyl)- 41 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 42 05 66.90% 5000

27 | 50 53 j__________ 71 37 +at TTTT T________ 85________ 101111111111022111132111 Tit I i i । i i i 111111j i.., । r...।..i. . ... ।..,. । | TTEgIui • ‘i' m/z—> 20 25 30 35 40 45 50 556065 70 7580859095 4.905.005.105.205.305.405.50

26393.D NP112701.M Tue Dec 04 10:43:47 2001 Page 2

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