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GCMS Analysis Report for Sample AD26389, Dec 2001

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Report documenting GCMS analysis of sample AD26389 with a note regarding unknown compounds.

NYC-WTC_000031473–000031490

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 Nov 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************** ** ** *************************** Peak Number 5 2-Butanol, 3-methyl-, (S)- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.19 4.44 ng/uL 1887330 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Butanol, 3-methyl-, (S) - 88 C5H120 001517-66-4 40 2 2-Butanol., 3-methyl- 88 C5H120 000598-75-4 9 3 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 4 Propane, 2-ethoxy-__________________ 88 C5H120 000625-54-7 9 Abundance Scan 256 (7.187 min): 26389.D (-) m/z 45.10 100.00% 45

5000 73 61 i . । i i r. । ri i i । . . > . j । । 6.80 7.00 7.20 7.40 7.60 1 +56 '—................................ — 41, --- . mamma 77 91 11] m/z 57.54% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #852:2-Butanol, 3-methyl-, (S)- 45

5000 • • I ‘ ‘ 6.80 7.00 7.20 7.40 7.60 m/z 73.05 40.11% 55 73

miz-> 20 27,31 mmp 25 30 35 M+ —1— 39

40 |

45 50 55 60 65 70 75 1 87 . . I I , I . I . , 11100111/1110717 1 | s > 1 r p 80 85 90 95 Abundance #62961:2-Butanol, 3-methyl- 45 V| i < t | » i r. j . i . ■ । . . . . । . 6.80 7.00 7.20 7.40 7.60 5000 m/z 61.00 38.50%

miz-> Abundance

5000 20 27 31 . munnpbuTTT1 .I ■ > ■ ।,। > |Nuunup 25 30 35 40 59 45

45 69 | 55 87 TTTETT r 8 "F 1 ‘ ' 1 TTT1—u 50 55 60 65 70 #62962: 2-Butanol, 3-methyl- 73

75 80 85 90 95

6.80 m/z 7.00 44.05 1 7.20 7.40 11.15% 7.60

55 73

m/z—> 20 2731 25 30 35 —4 —mnuua—Togm 40 45 50 55 60 65 | 88 ■ ■ ■ i1 ■1 ■ i ■ “118 8 “ i ■8" i 8 8 8 ■ i • • ■ • t8 70 75 80 85 90 95 6.80 7.00 7.20 7.40 7.60

26389.D NP112701.M Tue Dec 04 10:41:06 2001 Page 5

NYC-WTC_000031485

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NYC-WTC_000031485Source: NYC Law Department, mirrored locally

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