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GCMS analysis results for sample AD26681, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26681 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032079–000032092

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032088
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26681.D Vial: 2 Acq On 4 Dec 2001 11:44 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Butanol, 3-methyl-, (S)- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.15 3.25 ng/uL 1373010 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 2-Butane , 3-methyl-, (S)- 88 C5H120 001517-66-4 42 2 2-Butanol' , 3-methyl- 88 C5H120 000598-75-4 42 3 2,3 -Butanediol 90 C4H10O2 000513-85-9 33 4 2-Butanol, 3-methyl-____________ 88 C5H120 000598-75-4 33 Abundance Scan 251 (7.146 min): 26681.D (-) m/ z 45.10 100.00%| 45

5000- 61 73 MP 11 I P 1-1 1 • 1 1 1 1 1 J 6.80 7.00 7.20 7.40______ 207 I‘ 'I 1I '"'i1111 r -88 TTTTTTTTTTETTtIEEIETTTTTTTTT |.|ILf m/z 43.00 65.87% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #852: 2-Butanol, 3-methyl-, (S)- 45

5000- — = - J TT 6.80 7.00 7.20 7.40______ m/z 73.0,5 38.68% 27 73 55 1I 87 p' ‘'l'"‘I ।t i M | rl M | I i < i | i i | ■pTTTprrrrp-rr "I""I i" " i m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 Abundance #62961: 2-Butanol, 3-methyl- 45

6.80 7.00 7.20 7.40______ 5000 m/z 61.00 36.24%

73 55 27 87 f ■1'11 ICTTD p-m-p-TT 1‘‘‘‘9"111011 , Tp-my T‘"TTTTTTTTT‘TTT m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #917:2,3-Butanediol ____ .__________ II I ... I r... I .... I r 45 6.80 7.00 7.20 7.40______ m/z 44.05 1 3.68% 5000

29 I i .. 19 1 -H .1 57.1 ' ,l,,, T "'I' 75 90 --== — =====% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 6.80 7.00 7.20 7.40

26681.D NP112701.M Fri Dec 07 13:12:29 2001 Page 5

NYC-WTC_000032088

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NYC-WTC_000032088Source: NYC Law Department, mirrored locally

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