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GCMS analysis results for sample AD26681, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26681 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032079–000032092

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032087
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26681.D Vial: 2 Acq On 4 Dec 2001 11:44 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Furan, tetrahydro-2-(methoxyme Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.07 0.81 ng/uL 341598 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, tetrahydro- 2 - (methoxymethyl) 116 C6H12O2 019354-27-9 59 2 Borinic acid, diethyl-, methyl este 100 C5H13BO 007397-46-8 45 3 Furan, tetrahydro-2 - (methoxymethyl) 116 C6H1202 019354-27-9 45 4 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 40 'Abundance / Scan 134 (6.074 min): 26681.D (-) m/ z 71.05 100.00% ! ( 71

5000 43

57 5.80___6.00 6.20 6.40

m/z-> 10 20 30 — 40 —- 50 ll 60 70 4......... . 100............. m/z 43.05 46.35% I 80 90 100 110 120 Abundance #3276: Furan, tetrahydro-2-(methoxymethyl)- 71 43 5000 5.80 6.00 6.20 6.40 m/ Z 41.00 24.22% 27 I I 1— ’ 58 i

SM I *ndn-r//-1/1/1/1/111 116 ' I ■ ■ ■ ' i ■ ■ ' ■ i ■ r-j-rr-T-T-rr-T-r-T-f-r-r-r-r-^^ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1503: Borinic acid, diethyl-, methyl ester 71

43 - ' 5.80 6 00 6.20 6.40 5000 m/z 42.10 20.53% 15 27 ' ■ i ' 37 49 57 ' l I • ' I ' l I 85 100 m/z-> 10 'Abundance I 20 30 40 50 60 70 80 90 #64310: Furan, tetrahydro-2-(methoxymethyl)- 100 110 120 AAl AA 44AA 71 5.80 6.00 6.20 6.40 । m/z 70.05 10.69% 43 5000

58 m/z-> ------- 10 20 30 14 40 — 1 1 1 1 —r 50 60 70 80 85 90 116 ' i ' ' ' ' i • ' ' ■ i ' ■ ■ ■ i ' ■ ' ■ i ■ ■ 100 110 120 5.80 6.00 6.20 6.40

26681.D NP112701.M Fri Dec 07 13:12:27 2001 Page 4

NYC-WTC_000032087

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NYC-WTC_000032087Source: NYC Law Department, mirrored locally

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